Information card for entry 4078470

Structure parameters

• Formula: C38 H92 Cl9 O2 P4 Ru4
• Calculated formula: C38 H92 Cl9 O2 P4 Ru4
• Title of publication: Reactions of an Osmium(IV) Complex with Allenedienes: Coordination and Intramolecular Cycloadditions
• Authors of publication: Collado, Alba; Esteruelas, Miguel A.; Gulías, Moisés; Mascareñas, José L.; Oñate, Enrique
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 12
• Pages of publication: 4450
• a: 8.5966 ± 0.0011 Å
• b: 21.533 ± 0.003 Å
• c: 15.62 ± 0.002 Å
• α: 90°
• β: 102.284 ± 0.002°
• γ: 90°
• Cell volume: 2825.2 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 7
• Hermann-Mauguin space group symbol: P 1 c 1
• Hall space group symbol: P -2yc
• Residual factor for all reflections: 0.1047
• Residual factor for significantly intense reflections: 0.0738
• Weighted residual factors for significantly intense reflections: 0.171
• Weighted residual factors for all reflections included in the refinement: 0.1921
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No