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Information card for entry 4078494
Preview
Coordinates | 4078494.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C45 H40 Cl5 O4 P4 Pd Rh3 |
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Calculated formula | C45 H40 Cl5 O4 P4 Pd Rh3 |
SMILES | [Pd]123[Cl][Rh]4([Cl][Rh]([Cl]3)([P](C[P]1(CCC[P]2(C[P]4(c1ccccc1)c1ccccc1)c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)C#[O])C#[O].[Rh](Cl)(Cl)(C#[O])C#[O] |
Title of publication | Cyclic Trinuclear Rh2M Complexes (M = Rh, Pt, Pd, Ni) Supported bymeso-1,3-Bis[(diphenylphosphinomethyl)phenylphosphino]propane |
Authors of publication | Nakajima, Takayuki; Kurai, Sachi; Noda, Sayo; Zouda, Maki; Kure, Bunsho; Tanase, Tomoaki |
Journal of publication | Organometallics |
Year of publication | 2012 |
Journal volume | 31 |
Journal issue | 11 |
Pages of publication | 4283 |
a | 14.7507 ± 0.0011 Å |
b | 22.4667 ± 0.0014 Å |
c | 15.8882 ± 0.0013 Å |
α | 90° |
β | 113.48 ± 0.003° |
γ | 90° |
Cell volume | 4829.4 ± 0.6 Å3 |
Cell temperature | 153 ± 2 K |
Ambient diffraction temperature | 153 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for significantly intense reflections | 0.0376 |
Weighted residual factors for all reflections included in the refinement | 0.0772 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.88 |
Diffraction radiation wavelength | 0.71075 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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