Information card for entry 4078503

Structure parameters

• Formula: C63 H66 Cl11 F6 Hg N2 P5 Rh3
• Calculated formula: C63 H64 Cl11 F6 Hg N2 P5 Rh3
• Title of publication: Cyclic Trinuclear Rh2M Complexes (M = Rh, Pt, Pd, Ni) Supported bymeso-1,3-Bis[(diphenylphosphinomethyl)phenylphosphino]propane
• Authors of publication: Nakajima, Takayuki; Kurai, Sachi; Noda, Sayo; Zouda, Maki; Kure, Bunsho; Tanase, Tomoaki
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 11
• Pages of publication: 4283
• a: 10.069 ± 0.005 Å
• b: 40.207 ± 0.018 Å
• c: 17.987 ± 0.008 Å
• α: 90°
• β: 90.57 ± 0.004°
• γ: 90°
• Cell volume: 7282 ± 6 ų
• Cell temperature: 153 K
• Ambient diffraction temperature: 153 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0679
• Weighted residual factors for all reflections included in the refinement: 0.1902
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No