Information card for entry 4078539

Structure parameters

• Formula: C24 H48 Cl8 O12 Si8
• Calculated formula: C24 H48 Cl8 O12 Si8
• Title of publication: An Oligosilsesquioxane Cage Functionalized with Molybdenum(II) Organometallic Fragments
• Authors of publication: Dias Filho, Newton L.; Portugal, Fátima C. M.; Nogueira, J. M. F.; Brandão, Paula; Félix, Vitor; Vaz, Pedro D.; Nunes, Carla D.; Veiros, Luis F.; Brito, Maria J. Villa de; Calhorda, Maria José
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 12
• Pages of publication: 4495
• a: 10.2067 ± 0.0006 Å
• b: 15.2037 ± 0.0009 Å
• c: 15.5094 ± 0.0009 Å
• α: 99.157 ± 0.003°
• β: 103.552 ± 0.003°
• γ: 99.353 ± 0.003°
• Cell volume: 2259.3 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0928
• Residual factor for significantly intense reflections: 0.0585
• Weighted residual factors for significantly intense reflections: 0.1606
• Weighted residual factors for all reflections included in the refinement: 0.1908
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No