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Information card for entry 4078597
Preview
Coordinates | 4078597.cif |
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Original paper (by DOI) | HTML |
Formula | C21 H37 N3 Si |
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Calculated formula | C21 H37 N3 Si |
SMILES | [Si]1([N](=C(N1C(C)(C)C)c1ccccc1)C(C)(C)C)N(C(C)C)C(C)C |
Title of publication | Facile Access to the Functionalized N-Donor Stabilized Silylenes PhC(NtBu)2SiX (X = PPh2, NPh2, NCy2, NiPr2, NMe2, N(SiMe3)2, OtBu) |
Authors of publication | Azhakar, Ramachandran; Ghadwal, Rajendra S.; Roesky, Herbert W.; Wolf, Hilke; Stalke, Dietmar |
Journal of publication | Organometallics |
Year of publication | 2012 |
Journal volume | 31 |
Journal issue | 12 |
Pages of publication | 4588 |
a | 27.82 ± 0.002 Å |
b | 8.447 ± 0.003 Å |
c | 19.099 ± 0.002 Å |
α | 90° |
β | 99.35 ± 0.02° |
γ | 90° |
Cell volume | 4428.6 ± 1.7 Å3 |
Cell temperature | 101 ± 2 K |
Ambient diffraction temperature | 101 ± 2 K |
Number of distinct elements | 4 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0621 |
Residual factor for significantly intense reflections | 0.0416 |
Weighted residual factors for significantly intense reflections | 0.0936 |
Weighted residual factors for all reflections included in the refinement | 0.1002 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.047 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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