Information card for entry 4078651

Structure parameters

• Formula: C12 H30 Br2 O2 Si2 Sn
• Calculated formula: C12 H30 Br2 O2 Si2 Sn
• Title of publication: [Me2(i-PrO)SiCH2]2SnBr2: Evidence for Intramolecular Si‒O Bond Activation
• Authors of publication: Haj, Samer Baba; Schürmann, Markus; Iovkova-Berends, Ljuba; Herres-Pawlis, Sonja; Jurkschat, Klaus
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 13
• Pages of publication: 4716
• a: 13.6791 ± 0.0005 Å
• b: 29.6551 ± 0.001 Å
• c: 16.42 ± 0.0005 Å
• α: 90°
• β: 90.54 ± 0.003°
• γ: 90°
• Cell volume: 6660.6 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1221
• Residual factor for significantly intense reflections: 0.0472
• Weighted residual factors for significantly intense reflections: 0.1179
• Weighted residual factors for all reflections included in the refinement: 0.1371
• Goodness-of-fit parameter for all reflections included in the refinement: 0.683
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No