Information card for entry 4078700

Structure parameters

• Formula: C45 H50 Ag Au B F10 N12 O P
• Calculated formula: C45 H50 Ag Au B F10 N12 O P
• Title of publication: Gold(I), Gold(III), and Heterometallic Gold(I)‒Silver(I) and Gold(I)‒Copper(I) Complexes of a Pyridazine-Bridged NHC/Pyrazole Hybrid Ligand and Their Initial Application in Catalysis
• Authors of publication: Wimberg, Jan; Meyer, Steffen; Dechert, Sebastian; Meyer, Franc
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 14
• Pages of publication: 5025
• a: 37.4936 ± 0.0008 Å
• b: 14.7162 ± 0.0003 Å
• c: 26.6462 ± 0.0006 Å
• α: 90°
• β: 129.031 ± 0.001°
• γ: 90°
• Cell volume: 11420.9 ± 0.5 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 9
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0514
• Residual factor for significantly intense reflections: 0.0403
• Weighted residual factors for significantly intense reflections: 0.0987
• Weighted residual factors for all reflections included in the refinement: 0.1037
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No