Information card for entry 4078980
| Formula |
C43 H66 N10 Ti2 |
| Calculated formula |
C43 H66 N10 Ti2 |
| Title of publication |
Rapid Access to Substituted Piperazines via Ti(NMe2)4-Mediated C‒C Bond-Making Reactions |
| Authors of publication |
Chen, Zhou; Wu, Jian; Chen, Yanmei; Li, Lei; Xia, Yuanzhi; Li, Yahong; Liu, Wei; Lei, Tao; Yang, Lijuan; Gao, Dandan; Li, Wu |
| Journal of publication |
Organometallics |
| Year of publication |
2012 |
| Journal volume |
31 |
| Journal issue |
17 |
| Pages of publication |
6005 |
| a |
8.9558 ± 0.0007 Å |
| b |
12.3665 ± 0.001 Å |
| c |
12.5926 ± 0.0016 Å |
| α |
111.759 ± 0.006° |
| β |
103.185 ± 0.006° |
| γ |
106.276 ± 0.004° |
| Cell volume |
1154 ± 0.2 Å3 |
| Cell temperature |
296 ± 2 K |
| Ambient diffraction temperature |
296 ± 2 K |
| Number of distinct elements |
4 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.055 |
| Residual factor for significantly intense reflections |
0.0477 |
| Weighted residual factors for significantly intense reflections |
0.1382 |
| Weighted residual factors for all reflections included in the refinement |
0.1439 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.025 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
Yes |
| Has Fobs |
No |
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