Information card for entry 4079013

Structure parameters

• Formula: C66 H140 Cl2 Li2 N6 O4 Si8 Y2
• Calculated formula: C66 H140 Cl2 Li2 N6 O4 Si8 Y2
• Title of publication: Control of Conformations of Piperazidine-Bridged Bis(phenolato) Groups: Syntheses and Structures of Bimetallic and Monometallic Lanthanide Amides and Their Application in the Polymerization of Lactides
• Authors of publication: Li, Wenyi; Zhang, Zhongjian; Yao, Yingming; Zhang, Yong; Shen, Qi
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 9
• Pages of publication: 3499
• a: 11.6295 ± 0.0011 Å
• b: 12.8313 ± 0.0007 Å
• c: 16.4147 ± 0.0012 Å
• α: 75.22 ± 0.007°
• β: 88.127 ± 0.008°
• γ: 79.826 ± 0.007°
• Cell volume: 2330.9 ± 0.3 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0875
• Residual factor for significantly intense reflections: 0.0618
• Weighted residual factors for significantly intense reflections: 0.1326
• Weighted residual factors for all reflections included in the refinement: 0.1449
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No