Crystallography Open Database

Information card for entry 4079287

Preview

Coordinates	4079287.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H31 K N2 O Sn
Calculated formula	C20 H31 K N2 O Sn
Title of publication	Reactivity of a Distannylene toward Potassium Graphite: Synthesis of a Stannylidenide Anion
Authors of publication	Chia, Siew-Peng; Ganguly, Rakesh; Li, Yongxin; So, Cheuk-Wai
Journal of publication	Organometallics
Year of publication	2012
Journal volume	31
Journal issue	17
Pages of publication	6415
a	10.2822 ± 0.0005 Å
b	11.0911 ± 0.0005 Å
c	20.2384 ± 0.0012 Å
α	90°
β	90°
γ	90°
Cell volume	2308 ± 0.2 Å³
Cell temperature	103 ± 2 K
Ambient diffraction temperature	103 ± 2 K
Number of distinct elements	6
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0826
Residual factor for significantly intense reflections	0.0515
Weighted residual factors for significantly intense reflections	0.1055
Weighted residual factors for all reflections included in the refinement	0.1336
Goodness-of-fit parameter for all reflections included in the refinement	1.01
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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