Information card for entry 4079584

Structure parameters

• Formula: C39 H58 O3 Si W
• Calculated formula: C39 H58 O3 Si W
• Title of publication: Synthesis of Tungsten Oxo Alkylidene Complexes
• Authors of publication: Peryshkov, Dmitry V.; Schrock, Richard R.
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 20
• Pages of publication: 7278
• a: 9.3385 ± 0.001 Å
• b: 12.9036 ± 0.0014 Å
• c: 15.714 ± 0.0018 Å
• α: 91.207 ± 0.002°
• β: 92.359 ± 0.002°
• γ: 99.81 ± 0.002°
• Cell volume: 1863.5 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0338
• Residual factor for significantly intense reflections: 0.0255
• Weighted residual factors for significantly intense reflections: 0.0506
• Weighted residual factors for all reflections included in the refinement: 0.0531
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No