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Information card for entry 4079713
Preview
Coordinates | 4079713.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C49 H58 F2 N2 P2 Rh |
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Calculated formula | C49 H58 F2 N2 P2 Rh |
Title of publication | Ring-Expanded N-Heterocyclic Carbene Complexes of Rhodium with Bifluoride, Fluoride, and Fluoroaryl Ligands |
Authors of publication | Segarra, Candela; Mas-Marz Elena; Lowe, John P.; Mahon, Mary F.; Poulten, Rebecca C.; Whittlesey, Michael K. |
Journal of publication | Organometallics |
Year of publication | 2012 |
Journal volume | 31 |
Journal issue | 24 |
Pages of publication | 8584 |
a | 10.7914 ± 0.0003 Å |
b | 11.689 ± 0.0003 Å |
c | 18.7289 ± 0.0004 Å |
α | 75.783 ± 0.002° |
β | 86.843 ± 0.002° |
γ | 70.878 ± 0.002° |
Cell volume | 2162.93 ± 0.1 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0531 |
Residual factor for significantly intense reflections | 0.0333 |
Weighted residual factors for significantly intense reflections | 0.0699 |
Weighted residual factors for all reflections included in the refinement | 0.0727 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.935 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4079713.html
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Users of the data should acknowledge the original authors of the
structural data.