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Information card for entry 4079728
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Coordinates | 4079728.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | [Pd2(pentalene(SiiPr3)2)2] |
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Formula | C52 H92 Pd2 Si4 |
Calculated formula | C43.212 H76.452 Pd2 Si3.324 |
Title of publication | Double-Sandwich Pentalene Complexes M2(pent†)2(M = Rh, Pd; pent†= 1,4-Bis(triisopropylsilyl)pentalene): Synthesis, Structure, and Bonding |
Authors of publication | Summerscales, Owen T.; Rivers, Christopher J.; Taylor, Morgan J.; Hitchcock, Peter B.; Green, Jennifer C.; Cloke, F. Geoffrey N. |
Journal of publication | Organometallics |
Year of publication | 2012 |
Journal volume | 31 |
Journal issue | 24 |
Pages of publication | 8613 |
a | 21.374 ± 0.0012 Å |
b | 13.3834 ± 0.0008 Å |
c | 21.1553 ± 0.0012 Å |
α | 90° |
β | 96.549 ± 0.004° |
γ | 90° |
Cell volume | 6012.1 ± 0.6 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 4 |
Space group number | 5 |
Hermann-Mauguin space group symbol | C 1 2 1 |
Hall space group symbol | C 2y |
Residual factor for all reflections | 0.1155 |
Residual factor for significantly intense reflections | 0.1087 |
Weighted residual factors for significantly intense reflections | 0.2962 |
Weighted residual factors for all reflections included in the refinement | 0.3021 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.135 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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