Information card for entry 4079795

Structure parameters

• Formula: C105 H100 Ag2 Cu2 F20 Ge2 N4
• Calculated formula: C105 H92 Ag2 Cu2 F20 Ge2 N4
• Title of publication: Reactivity Studies of (Phenylethynyl)germylene LGeC≡CPh (L = HC[C(Me)N-2,6-iPr2C6H3]2) toward Pentafluorophenylcopper(I), -silver(I), and -gold(I) Complexes
• Authors of publication: Zhao, Na; Zhang, Jinyuan; Yang, Ying; Chen, Guifang; Zhu, Hongping; Roesky, Herbert W.
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 3
• Pages of publication: 762
• a: 12.1485 ± 0.0006 Å
• b: 14.5308 ± 0.0005 Å
• c: 15.7442 ± 0.0008 Å
• α: 71.045 ± 0.004°
• β: 69.256 ± 0.005°
• γ: 70.946 ± 0.004°
• Cell volume: 2386.9 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.089
• Residual factor for significantly intense reflections: 0.0704
• Weighted residual factors for significantly intense reflections: 0.1792
• Weighted residual factors for all reflections included in the refinement: 0.1907
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No