fac-Re(CO)3Cl Complexes of [2-(4-R-1H-1,2,3-Triazol-1-yl)methyl]pyridine Inverse “Click” Ligands: A Systematic Synthetic, Spectroscopic, and Computational Study
Authors of publication
Anderson, Christopher B.; Elliott, Anastasia B. S.; McAdam, C. John; Gordon, Keith C.; Crowley, James D.
Journal of publication
Organometallics
Year of publication
2013
Journal volume
32
Journal issue
3
Pages of publication
788
a
7.5568 ± 0.0006 Å
b
9.5664 ± 0.0009 Å
c
13.4313 ± 0.0012 Å
α
84.932 ± 0.004°
β
83.901 ± 0.004°
γ
69.692 ± 0.004°
Cell volume
904.08 ± 0.14 Å3
Cell temperature
89 ± 2 K
Ambient diffraction temperature
89 ± 2 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0377
Residual factor for significantly intense reflections
0.0341
Weighted residual factors for significantly intense reflections
0.0921
Weighted residual factors for all reflections included in the refinement
0.1031
Goodness-of-fit parameter for all reflections included in the refinement
