Information card for entry 4079896

Structure parameters

• Common name: Pb(ONO-Q)2 . 2 CHCl3
• Chemical name: Bis[2-(3,5-di-tert-butyl-o-quinoneiminato)-4,6-di-tert- butylphenoxy]lead(II) dichloroform solvate
• Formula: C58 H82 Cl6 N2 O4 Pb
• Calculated formula: C58 H82 Cl6 N2 O4 Pb
• Title of publication: Migrations of Alkyl and Aryl Groups from Silicon to Nitrogen in Silylated Aryloxyiminoquinones
• Authors of publication: Shekar, Sukesh; Brown, Seth N.
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 2
• Pages of publication: 556
• a: 11.1201 ± 0.0011 Å
• b: 12.8168 ± 0.0015 Å
• c: 23.1726 ± 0.0019 Å
• α: 103.694 ± 0.007°
• β: 90.075 ± 0.005°
• γ: 106.822 ± 0.007°
• Cell volume: 3062.8 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0377
• Residual factor for significantly intense reflections: 0.0299
• Weighted residual factors for significantly intense reflections: 0.0633
• Weighted residual factors for all reflections included in the refinement: 0.0662
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No