Information card for entry 4079961

Structure parameters

• Common name: 8Pd
• Formula: C23 H41 F3 N O3 P Pd S
• Calculated formula: C23 H41 F3 N O3 P Pd S
• Title of publication: Investigation of Steric and Electronic Features of 3-Iminophosphine-Based Palladium Catalysts for Intermolecular Hydroamination
• Authors of publication: Zingales, Nicholas C.; Shaffer, Andrew R.; Schmidt, Joseph A. R.
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 2
• Pages of publication: 578
• a: 10.315 ± 0.002 Å
• b: 10.453 ± 0.002 Å
• c: 13.04 ± 0.003 Å
• α: 73.83 ± 0.03°
• β: 79.74 ± 0.03°
• γ: 84.99 ± 0.03°
• Cell volume: 1327.7 ± 0.5 ų
• Cell temperature: 140 ± 2 K
• Ambient diffraction temperature: 140 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.076
• Residual factor for significantly intense reflections: 0.0696
• Weighted residual factors for significantly intense reflections: 0.1881
• Weighted residual factors for all reflections included in the refinement: 0.1923
• Goodness-of-fit parameter for all reflections included in the refinement: 1.172
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No