Information card for entry 4079984

Structure parameters

• Formula: C48 H51 F Ge
• Calculated formula: C48 H51 F Ge
• Title of publication: Facile, High-Yield Functionalization of Germanium and Tin by Oxidative Insertion of Tetrelenes into the E‒H Bonds of Inorganic Acids (E = C, N, O, F): Arene Elimination versus Oxidative Addition and Formation of a Germanium Cation‒Water Complex
• Authors of publication: Brown, Zachary D.; Erickson, Jeremy D.; Fettinger, James C.; Power, Philip P.
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 2
• Pages of publication: 617
• a: 20.782 ± 0.004 Å
• b: 44.041 ± 0.009 Å
• c: 8.2142 ± 0.0014 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7518 ± 2 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 4
• Space group number: 43
• Hermann-Mauguin space group symbol: F d d 2
• Hall space group symbol: F 2 -2d
• Residual factor for all reflections: 0.0388
• Residual factor for significantly intense reflections: 0.0357
• Weighted residual factors for significantly intense reflections: 0.0865
• Weighted residual factors for all reflections included in the refinement: 0.0884
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No