Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4080051
Preview
Coordinates | 4080051.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C58.5 H71 N9 Zr |
---|---|
Calculated formula | C58.5 H71 N9 Zr |
Title of publication | Zirconium Hydrazinediido Complexes Derived from Cyclic Hydrazines and Their Role in the Catalytic Synthesis of 1,7-Annulated Indoles |
Authors of publication | Scholl, Solveig A.; Wadepohl, Hubert; Gade, Lutz H. |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 3 |
Pages of publication | 937 |
a | 18.8426 ± 0.0002 Å |
b | 15.35907 ± 0.00016 Å |
c | 18.8516 ± 0.0002 Å |
α | 90° |
β | 105.363 ± 0.0013° |
γ | 90° |
Cell volume | 5260.8 ± 0.1 Å3 |
Cell temperature | 114.97 ± 0.11 K |
Ambient diffraction temperature | 114.97 ± 0.11 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0448 |
Residual factor for significantly intense reflections | 0.0331 |
Weighted residual factors for significantly intense reflections | 0.074 |
Weighted residual factors for all reflections included in the refinement | 0.0795 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.024 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.5418 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4080051.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.