Information card for entry 4080074

Structure parameters

• Formula: C54 H48 P2 Pd Si4
• Calculated formula: C54 H48 P2 Pd Si4
• SMILES: c12ccccc2c2c(cccc2)[Si]21[Pd]1([P](C)(C)CC[P]1(C)C)[Si]1(c3c(cccc3)c3c1cccc3)[Si]1([Si]32c2c(cccc2)c2c3cccc2)c2c(cccc2)c2c1cccc2
• Title of publication: Nickel-Catalyzed Cyclopolymerization of Hexyl- and Phenylsilanes
• Authors of publication: Tanabe, Makoto; Takahashi, Atsushi; Fukuta, Tomoko; Osakada, Kohtaro
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 4
• Pages of publication: 1037
• a: 14.447 ± 0.003 Å
• b: 14.447 ± 0.003 Å
• c: 22.606 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4718.2 ± 1.7 ų
• Cell temperature: 113 K
• Ambient diffraction temperature: 113 K
• Number of distinct elements: 5
• Space group number: 86
• Hermann-Mauguin space group symbol: P 42/n :2
• Hall space group symbol: -P 4bc
• Residual factor for significantly intense reflections: 0.0439
• Weighted residual factors for all reflections included in the refinement: 0.1097
• Goodness-of-fit parameter for all reflections included in the refinement: 1.122
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No