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Information card for entry 4080093
Preview
Coordinates | 4080093.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C44 H72 Ge O2.5 P |
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Calculated formula | C44 H72 Ge O2.5 P |
Title of publication | Versatile Reactivity of Phosphagermaallene Tip(t-Bu)Ge═C═PMes* with α-Ethylenic Esters |
Authors of publication | Ghereg, Dumitru; Ouhsaine, Fatima; Escudié, Jean; Labat, Stéphane; André, Erwan; Miqueu, Karinne; Sotiropoulos, Jean-Marc; Gornitzka, Heinz; Saffon, Nathalie |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 4 |
Pages of publication | 1085 |
a | 14.8991 ± 0.0004 Å |
b | 18.2616 ± 0.0005 Å |
c | 16.6892 ± 0.0004 Å |
α | 90° |
β | 104.424 ± 0.002° |
γ | 90° |
Cell volume | 4397.7 ± 0.2 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0803 |
Residual factor for significantly intense reflections | 0.0422 |
Weighted residual factors for significantly intense reflections | 0.083 |
Weighted residual factors for all reflections included in the refinement | 0.0967 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.005 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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