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Information card for entry 4080121
Preview
Coordinates | 4080121.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C56 H60 K2 N2 P4 S2 Si2 |
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Calculated formula | C56 H60 K2 N2 P4 S2 Si2 |
SMILES | [K+].N(=P(C=P([S-])(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)[Si](C)(C)C |
Title of publication | (Iminophosphoranyl)(thiophosphoranyl)methanide {CH(PPh2NSiMe3)(Ph2PS)}−as a Ligand in Rare-Earth-Element Chemistry |
Authors of publication | Murugesapandian, Balasubramanian; Kuzdrowska, Magdalena; Gamer, Michael T.; Hartenstein, Larissa; Roesky, Peter W. |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 5 |
Pages of publication | 1500 - 1506 |
a | 11.5785 ± 0.0005 Å |
b | 14.3272 ± 0.0005 Å |
c | 16.7733 ± 0.0008 Å |
α | 90° |
β | 97.621 ± 0.004° |
γ | 90° |
Cell volume | 2757.9 ± 0.2 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0898 |
Residual factor for significantly intense reflections | 0.0403 |
Weighted residual factors for significantly intense reflections | 0.0501 |
Weighted residual factors for all reflections included in the refinement | 0.057 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.803 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4080121.html
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