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Information card for entry 4080124
Preview
Coordinates | 4080124.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C36 H58 N3 P2 S Si5 Y |
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Calculated formula | C36 H58 N3 P2 S Si5 Y |
Title of publication | (Iminophosphoranyl)(thiophosphoranyl)methanide {CH(PPh2NSiMe3)(Ph2PS)}−as a Ligand in Rare-Earth-Element Chemistry |
Authors of publication | Murugesapandian, Balasubramanian; Kuzdrowska, Magdalena; Gamer, Michael T.; Hartenstein, Larissa; Roesky, Peter W. |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 5 |
Pages of publication | 1500 - 1506 |
a | 17.9574 ± 0.0008 Å |
b | 18.1055 ± 0.0005 Å |
c | 28.2892 ± 0.001 Å |
α | 90° |
β | 92.465 ± 0.003° |
γ | 90° |
Cell volume | 9189.1 ± 0.6 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 7 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.1297 |
Residual factor for significantly intense reflections | 0.0548 |
Weighted residual factors for significantly intense reflections | 0.0717 |
Weighted residual factors for all reflections included in the refinement | 0.0865 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.803 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4080124.html
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