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Information card for entry 4080142
Preview
Coordinates | 4080142.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C21 H37 Al2 N2 Y |
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Calculated formula | C21 H37 Al2 N2 Y |
SMILES | [Y]123([CH3][Al]([CH3]2)(C)C)([CH3][Al]([CH3]3)(C)C)n2cccc2C=[N]1c1c(cccc1C)C |
Title of publication | Synthesis of Rare-Earth-Metal Iminopyrrolyl Complexes from Alkyl Precursors: Ln→Al N-Ancillary Ligand Transfer |
Authors of publication | Kaneko, Hiroshi; Dietrich, H. Martin; Schädle, Christoph; Maichle-Mössmer, Cäcilia; Tsurugi, Hayato; Törnroos, Karl W.; Mashima, Kazushi; Anwander, Reiner |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 5 |
Pages of publication | 1199 |
a | 9.2848 ± 0.0003 Å |
b | 11.5466 ± 0.0004 Å |
c | 12.5982 ± 0.0005 Å |
α | 105.821 ± 0.001° |
β | 106.197 ± 0.001° |
γ | 93.899 ± 0.001° |
Cell volume | 1232.62 ± 0.08 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0227 |
Residual factor for significantly intense reflections | 0.0198 |
Weighted residual factors for significantly intense reflections | 0.0509 |
Weighted residual factors for all reflections included in the refinement | 0.052 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.081 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4080142.html
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