Information card for entry 4080171

Structure parameters

• Common name: {[Me3NN]Ni}2(m-CO)2
• Formula: C24 H29 N2 Ni O
• Calculated formula: C24 H29 N2 Ni O
• Title of publication: β-Diketiminato Nickel Imides in Catalytic Nitrene Transfer to Isocyanides
• Authors of publication: Wiese, Stefan; Aguila, Mae Joanne B.; Kogut, Elzbieta; Warren, Timothy H.
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 8
• Pages of publication: 2300
• a: 22.103 ± 0.015 Å
• b: 8.942 ± 0.009 Å
• c: 22.82 ± 0.02 Å
• α: 90°
• β: 108.48 ± 0.03°
• γ: 90°
• Cell volume: 4278 ± 6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1095
• Residual factor for significantly intense reflections: 0.0511
• Weighted residual factors for significantly intense reflections: 0.1201
• Weighted residual factors for all reflections included in the refinement: 0.1355
• Goodness-of-fit parameter for all reflections included in the refinement: 0.967
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No