Information card for entry 4080292

Structure parameters

• Common name: complex_8
• Formula: C38 H67 Si2 U
• Calculated formula: C38 H67 Si2 U
• Title of publication: Steric Effects in the Reductive Coupling of CO by Mixed-Sandwich Uranium(III) Complexes
• Authors of publication: Tsoureas, Nikolaos; Summerscales, Owen T.; Cloke, F. Geoffrey N.; Roe, S. Mark
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 5
• Pages of publication: 1353
• a: 11.9814 ± 0.0002 Å
• b: 15.207 ± 0.0003 Å
• c: 21.7406 ± 0.0005 Å
• α: 90°
• β: 90.008 ± 0.001°
• γ: 90°
• Cell volume: 3961.16 ± 0.14 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0904
• Residual factor for significantly intense reflections: 0.0454
• Weighted residual factors for significantly intense reflections: 0.0696
• Weighted residual factors for all reflections included in the refinement: 0.078
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No