Information card for entry 4080295

Structure parameters

• Common name: complex_12
• Formula: C86 H151.3 O2 Si4 U2
• Calculated formula: C86 H151.304 O2 Si4 U2
• Title of publication: Steric Effects in the Reductive Coupling of CO by Mixed-Sandwich Uranium(III) Complexes
• Authors of publication: Tsoureas, Nikolaos; Summerscales, Owen T.; Cloke, F. Geoffrey N.; Roe, S. Mark
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 5
• Pages of publication: 1353
• a: 11.197 ± 0.002 Å
• b: 14.297 ± 0.003 Å
• c: 15.97 ± 0.003 Å
• α: 66.38 ± 0.03°
• β: 70.6 ± 0.03°
• γ: 85.91 ± 0.03°
• Cell volume: 2203.7 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0574
• Residual factor for significantly intense reflections: 0.0404
• Weighted residual factors for significantly intense reflections: 0.0783
• Weighted residual factors for all reflections included in the refinement: 0.0852
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No