Information card for entry 4080297

Structure parameters

• Common name: complex_15
• Formula: C26 H33 O2 Si2 U
• Calculated formula: C26 H33 O2 Si2 U
• Title of publication: Steric Effects in the Reductive Coupling of CO by Mixed-Sandwich Uranium(III) Complexes
• Authors of publication: Tsoureas, Nikolaos; Summerscales, Owen T.; Cloke, F. Geoffrey N.; Roe, S. Mark
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 5
• Pages of publication: 1353
• a: 12.067 ± 0.002 Å
• b: 13.795 ± 0.003 Å
• c: 17.212 ± 0.003 Å
• α: 90°
• β: 100.83 ± 0.03°
• γ: 90°
• Cell volume: 2814.2 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0827
• Residual factor for significantly intense reflections: 0.048
• Weighted residual factors for significantly intense reflections: 0.1027
• Weighted residual factors for all reflections included in the refinement: 0.1194
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No