Information card for entry 4080306

Structure parameters

• Common name: [Sm(DippForm)2(OCH=CH2)(THF)]
• Formula: C56 H81 N4 O2 Sm
• Calculated formula: C56 H81 N4 O2 Sm
• Title of publication: Bulky Formamidinate-Supported Lanthanoid Halides and Alkyls, Including a Rare Terminal La‒Me Species
• Authors of publication: Cole, Marcus L.; Deacon, Glen B.; Junk, Peter C.; Wang, Jun
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 5
• Pages of publication: 1370
• a: 12.2755 ± 0.0003 Å
• b: 14.0703 ± 0.0003 Å
• c: 17.8816 ± 0.0005 Å
• α: 78.315 ± 0.001°
• β: 69.943 ± 0.001°
• γ: 67.892 ± 0.001°
• Cell volume: 2678.3 ± 0.12 ų
• Cell temperature: 123 ± 1 K
• Ambient diffraction temperature: 123 ± 1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0432
• Residual factor for significantly intense reflections: 0.0367
• Weighted residual factors for significantly intense reflections: 0.078
• Weighted residual factors for all reflections included in the refinement: 0.0825
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No