Diamine Bis(phenolate) as Supporting Ligands in Organoactinide(IV) Chemistry. Synthesis, Structural Characterization, and Reactivity of Stable Dialkyl Derivatives
Authors of publication
Mora, Elsa; Maria, Leonor; Biswas, Biplab; Camp, Clément; Santos, Isabel C.; Pécaut, Jacques; Cruz, Adelaide; Carretas, José M.; Marçalo, Joaquim; Mazzanti, Marinella
Journal of publication
Organometallics
Year of publication
2013
Journal volume
32
Journal issue
5
Pages of publication
1409
a
18.2767 ± 0.0003 Å
b
24.4463 ± 0.0004 Å
c
16.6782 ± 0.0003 Å
α
90°
β
99.62 ± 0.001°
γ
90°
Cell volume
7347 ± 0.2 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
5
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.0357
Residual factor for significantly intense reflections
0.0309
Weighted residual factors for significantly intense reflections
0.0821
Weighted residual factors for all reflections included in the refinement
0.0838
Goodness-of-fit parameter for all reflections included in the refinement
