Information card for entry 4080429

Structure parameters

• Formula: C38 H60 Fe2 N2 Si4
• Calculated formula: C38 H60 Fe2 N2 Si4
• Title of publication: Disilametallacycles as a Platform for Stabilizing M(II) and M(IV) (M = Fe, Ru) Centers: Synthesis and Characterization of Half-Sandwich Complexes and Their Application to Catalytic Double Silylation of Alkenes and Alkynes
• Authors of publication: Sunada, Yusuke; Imaoka, Tsuyoshi; Nagashima, Hideo
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 7
• Pages of publication: 2112
• a: 14.4983 ± 0.0018 Å
• b: 14.8867 ± 0.0017 Å
• c: 10.594 ± 0.0014 Å
• α: 90°
• β: 125.259 ± 0.003°
• γ: 90°
• Cell volume: 1867.1 ± 0.4 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 5
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for significantly intense reflections: 0.0487
• Weighted residual factors for all reflections included in the refinement: 0.1891
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No