Information card for entry 4080432

Structure parameters

• Formula: C48 H96 P2 Pd2 Si2
• Calculated formula: C48 H96 P2 Pd2 Si2
• Title of publication: Dipalladium Complexes with Bridging Monoalkyl or Monophenyl Silyl Ligands in the Solid State and in Solution
• Authors of publication: Tanabe, Makoto; Takahashi, Atsushi; Yamada, Tetsuyuki; Osakada, Kohtaro
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 6
• Pages of publication: 1815
• a: 8.75 ± 0.003 Å
• b: 12.045 ± 0.003 Å
• c: 13.198 ± 0.004 Å
• α: 101.664 ± 0.004°
• β: 108.563 ± 0.004°
• γ: 93.812 ± 0.0013°
• Cell volume: 1278.5 ± 0.7 ų
• Cell temperature: 113 K
• Ambient diffraction temperature: 113 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0724
• Residual factor for significantly intense reflections: 0.0603
• Weighted residual factors for significantly intense reflections: 0.1662
• Weighted residual factors for all reflections included in the refinement: 0.1798
• Goodness-of-fit parameter for all reflections included in the refinement: 1.094
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No