Information card for entry 4080434

Structure parameters

• Formula: C48 H78 Cl2 P2 Pd2 Si2
• Calculated formula: C48 H78 Cl2 P2 Pd2 Si2
• SMILES: [Pd]123([Pd]4([P](C5CCCCC5)(C5CCCCC5)C5CCCCC5)([Si]1(Cl)(c1ccccc1)[H]3)[Si]2(Cl)(c1ccccc1)[H]4)[P](C1CCCCC1)(C1CCCCC1)C1CCCCC1
• Title of publication: Dipalladium Complexes with Bridging Monoalkyl or Monophenyl Silyl Ligands in the Solid State and in Solution
• Authors of publication: Tanabe, Makoto; Takahashi, Atsushi; Yamada, Tetsuyuki; Osakada, Kohtaro
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 6
• Pages of publication: 1815
• a: 11.969 ± 0.004 Å
• b: 22.797 ± 0.006 Å
• c: 18.311 ± 0.006 Å
• α: 90°
• β: 95.378 ± 0.005°
• γ: 90°
• Cell volume: 4974 ± 3 ų
• Cell temperature: 113 K
• Ambient diffraction temperature: 113 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1012
• Residual factor for significantly intense reflections: 0.0729
• Weighted residual factors for significantly intense reflections: 0.1972
• Weighted residual factors for all reflections included in the refinement: 0.2268
• Goodness-of-fit parameter for all reflections included in the refinement: 1.114
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No