Information card for entry 4080472

Structure parameters

• Formula: C52 H87 Cl N6 Si4 Yb2
• Calculated formula: C52 H87 Cl N6 Si4 Yb2
• Title of publication: Unexpected C‒H Bond Activation Promoted by Bimetallic Lanthanide Amido Complexes Bearing a META-Phenylene-Bridged Bis(β-diketiminate) Ligand
• Authors of publication: Sun, Song; Sun, Qiu; Zhao, Bei; Zhang, Yong; Shen, Qi; Yao, Yingming
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 6
• Pages of publication: 1876
• a: 11.4491 ± 0.001 Å
• b: 11.927 ± 0.0011 Å
• c: 24.1294 ± 0.0019 Å
• α: 92.904 ± 0.002°
• β: 92.422 ± 0.002°
• γ: 114.028 ± 0.002°
• Cell volume: 2998.4 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0646
• Residual factor for significantly intense reflections: 0.0524
• Weighted residual factors for significantly intense reflections: 0.1207
• Weighted residual factors for all reflections included in the refinement: 0.1315
• Goodness-of-fit parameter for all reflections included in the refinement: 1.097
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No