Information card for entry 4080505

Structure parameters

• Formula: C60 H58 B F24 P Ru
• Calculated formula: C60 H58 B F24 P Ru
• Title of publication: Aminoborane σ Complexes: Significance of Hydride Co-ligands in Dynamic Processes and Dehydrogenative Borylene Formation
• Authors of publication: Addy, David A.; Bates, Joshua I.; Kelly, Michael J.; Riddlestone, Ian M.; Aldridge, Simon
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 6
• Pages of publication: 1583
• a: 18.9717 ± 0.0001 Å
• b: 17.2717 ± 0.0001 Å
• c: 36.3666 ± 0.0003 Å
• α: 90°
• β: 94.5427 ± 0.0003°
• γ: 90°
• Cell volume: 11878.9 ± 0.14 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1168
• Residual factor for significantly intense reflections: 0.0733
• Weighted residual factors for all reflections: 0.1915
• Weighted residual factors for significantly intense reflections: 0.1694
• Weighted residual factors for all reflections included in the refinement: 0.1915
• Goodness-of-fit parameter for all reflections included in the refinement: 0.928
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No