Information card for entry 4080536

Structure parameters

• Formula: C51 H53 Cl4 N3 W Zn
• Calculated formula: C51 H53 Cl4 N3 W Zn
• Title of publication: Molybdenum and Tungsten Monoalkoxide Pyrrolide (MAP) Alkylidene Complexes That Contain a 2,6-Dimesitylphenylimido Ligand
• Authors of publication: Gerber, Laura C. H.; Schrock, Richard R.; Müller, Peter
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 8
• Pages of publication: 2373
• a: 9.883 ± 0.0007 Å
• b: 11.6031 ± 0.0008 Å
• c: 20.9756 ± 0.0015 Å
• α: 79.475 ± 0.002°
• β: 83.237 ± 0.001°
• γ: 83.253 ± 0.002°
• Cell volume: 2337 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0307
• Residual factor for significantly intense reflections: 0.0261
• Weighted residual factors for significantly intense reflections: 0.063
• Weighted residual factors for all reflections included in the refinement: 0.0644
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No