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Information card for entry 4080605
Preview
Coordinates | 4080605.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | [K(18-crown-6)][As3C2PhH]*THF |
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Formula | C24 H38 As3 K O7 |
Calculated formula | C24 H38 As3 K O7 |
Title of publication | Synthesis and Characterization of Free and Coordinated 1,2,3-Tripnictolide Anions |
Authors of publication | Turbervill, Robert S. P.; Jupp, Andrew R.; McCullough, Phillip S. B.; Ergöçmen, Doruk; Goicoechea, Jose M. |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 7 |
Pages of publication | 2234 |
a | 8.0614 ± 0.0002 Å |
b | 10.1857 ± 0.0002 Å |
c | 19.1222 ± 0.0004 Å |
α | 94.17 ± 0.002° |
β | 96.314 ± 0.002° |
γ | 106.266 ± 0.002° |
Cell volume | 1489.31 ± 0.06 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0269 |
Residual factor for significantly intense reflections | 0.0261 |
Weighted residual factors for significantly intense reflections | 0.0708 |
Weighted residual factors for all reflections included in the refinement | 0.0717 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.05 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4080605.html
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