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Information card for entry 4080677
Preview
Coordinates | 4080677.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C27 H59 Cl O3 Os P2 |
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Calculated formula | C27 H59 Cl O3 Os P2 |
SMILES | [OsH2]1(Cl)([P](C(C)C)(C(C)C)C(C)C)([P](C(C)C)(C(C)C)C(C)C)[O]=C(C=C1C)OCC.O=C(C)C |
Title of publication | Hydroosmiation of Allenes and Reductive Elimination of Olefin in Unsaturated Osmium(IV) Polyhydrides: Hydride versus Chloride |
Authors of publication | Esteruelas, Miguel A.; Larramona, Carmen; Oñate, Enrique |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 9 |
Pages of publication | 2567 |
a | 8.7675 ± 0.001 Å |
b | 11.8843 ± 0.0014 Å |
c | 16.7509 ± 0.0019 Å |
α | 98.151 ± 0.002° |
β | 100.785 ± 0.002° |
γ | 104.551 ± 0.001° |
Cell volume | 1626.5 ± 0.3 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0265 |
Residual factor for significantly intense reflections | 0.0226 |
Weighted residual factors for significantly intense reflections | 0.0494 |
Weighted residual factors for all reflections included in the refinement | 0.0506 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.029 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4080677.html
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