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Information card for entry 4080850
Preview
Coordinates | 4080850.cif |
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Original paper (by DOI) | HTML |
Common name | oemw [W(PNP-iPr)(CO)3].THF.1/2hexane (5b.THF.1/2hexane) |
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Chemical name | [W(PNP-iPr)(CO)3].THF.1/2hexane (5b.THF.1/2hexane) |
Formula | C27 H48 N3 O4 P2 W |
Calculated formula | C24 H41 N3 O4 P2 W |
Title of publication | Synthesis and Characterization of Hydrido Carbonyl Molybdenum and Tungsten PNP Pincer Complexes. |
Authors of publication | Oztopcu, Ozgür; Holzhacker, Christian; Puchberger, Michael; Weil, Matthias; Mereiter, Kurt; Veiros, Luis F.; Kirchner, Karl |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 10 |
Pages of publication | 3042 - 3052 |
a | 10.1399 ± 0.001 Å |
b | 15.5053 ± 0.0018 Å |
c | 20.036 ± 0.002 Å |
α | 90° |
β | 94.485 ± 0.005° |
γ | 90° |
Cell volume | 3140.5 ± 0.6 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0689 |
Residual factor for significantly intense reflections | 0.0398 |
Weighted residual factors for significantly intense reflections | 0.0805 |
Weighted residual factors for all reflections included in the refinement | 0.0907 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.046 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4080850.html
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