Information card for entry 4080883

Structure parameters

• Chemical name: Ti(N2ArO)(NNPh2)(bipy_tBu)
• Formula: C51.5 H64 N6 O Si2 Ti
• Calculated formula: C51.5 H64 N6 O Si2 Ti
• Title of publication: Synthesis and Reactivity of Titanium Hydrazido Complexes Supported by Diamido-Ether Ligands
• Authors of publication: Unruangsri, Junjuda; Morgan, Hannah; Schwarz, Andrew D.; Schofield, A. Daniel; Mountford, Philip
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 10
• Pages of publication: 3091
• a: 11.2543 ± 0.0003 Å
• b: 13.2633 ± 0.0003 Å
• c: 19.3767 ± 0.0005 Å
• α: 91.2 ± 0.001°
• β: 101.007 ± 0.0011°
• γ: 107.604 ± 0.0011°
• Cell volume: 2696.59 ± 0.12 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1421
• Residual factor for significantly intense reflections: 0.0982
• Weighted residual factors for all reflections: 0.1333
• Weighted residual factors for significantly intense reflections: 0.0986
• Weighted residual factors for all reflections included in the refinement: 0.0931
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No