Information card for entry 4080910

Structure parameters

• Formula: C40 H42 Ge2 O3 Si2
• Calculated formula: C40 H42 Ge2 O3 Si2
• Title of publication: (Me3N)Mo(CO)5-Catalyzed Reduction of DMF by Disiloxane and Disilane Moieties: Fate of the Silicon-Containing Fragments
• Authors of publication: Sharma, Hemant K.; Arias-Ugarte, Renzo; Tomlinson, David; Gappa, Rie; Metta-Maga Alejandro J.; Ito, Haruhiko; Pannell, Keith H.
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 14
• Pages of publication: 3788
• a: 9 ± 0.005 Å
• b: 11.516 ± 0.006 Å
• c: 19.784 ± 0.011 Å
• α: 97.966 ± 0.01°
• β: 97.355 ± 0.01°
• γ: 94.346 ± 0.009°
• Cell volume: 2004.8 ± 1.9 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1217
• Residual factor for significantly intense reflections: 0.0501
• Weighted residual factors for significantly intense reflections: 0.1184
• Weighted residual factors for all reflections included in the refinement: 0.151
• Goodness-of-fit parameter for all reflections included in the refinement: 0.733
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No