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Information card for entry 4080948
Preview
Coordinates | 4080948.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C143 H166 B2 F38 N2 P4 Pd2 |
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Calculated formula | C143 H158 B2 F38 N2 P4 Pd2 |
Title of publication | Carbon‒Fluorine Bond Activation of Tetrafluoroethylene on Palladium(0) and Nickel(0): Heat or Lewis Acidic Additive Promoted Oxidative Addition |
Authors of publication | Ohashi, Masato; Shibata, Mitsutoshi; Saijo, Hiroki; Kambara, Tadashi; Ogoshi, Sensuke |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 13 |
Pages of publication | 3631 |
a | 11.8512 ± 0.0007 Å |
b | 13.2993 ± 0.0007 Å |
c | 22.5605 ± 0.0013 Å |
α | 83.157 ± 0.002° |
β | 76.718 ± 0.001° |
γ | 88.021 ± 0.001° |
Cell volume | 3436 ± 0.3 Å3 |
Cell temperature | 123 ± 2 K |
Ambient diffraction temperature | 123 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0548 |
Residual factor for significantly intense reflections | 0.0422 |
Weighted residual factors for significantly intense reflections | 0.0997 |
Weighted residual factors for all reflections included in the refinement | 0.1078 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.033 |
Diffraction radiation wavelength | 0.71075 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4080948.html
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