Information card for entry 4081053

Structure parameters

• Formula: C198 H234 N2 O6 Si6 U2
• Calculated formula: C198 H234 N2 O6 Si6 U2
• Title of publication: Thermally Stable Uranium Dinitrogen Complex with Siloxide Supporting Ligands
• Authors of publication: Mansell, Stephen M.; Farnaby, Joy H.; Germeroth, Anne I.; Arnold, Polly L.
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 15
• Pages of publication: 4214
• a: 38.9299 ± 0.0014 Å
• b: 18.1633 ± 0.0003 Å
• c: 29.0426 ± 0.0009 Å
• α: 90°
• β: 120.871 ± 0.005°
• γ: 90°
• Cell volume: 17626.5 ± 1.3 ų
• Cell temperature: 170 ± 2 K
• Ambient diffraction temperature: 170 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0789
• Residual factor for significantly intense reflections: 0.0424
• Weighted residual factors for significantly intense reflections: 0.1051
• Weighted residual factors for all reflections included in the refinement: 0.1125
• Goodness-of-fit parameter for all reflections included in the refinement: 0.966
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No