Information card for entry 4081056

Structure parameters

• Formula: C130.27 H177.06 O4 Si4 U
• Calculated formula: C130.277 H177.055 O4 Si4 U
• Title of publication: Thermally Stable Uranium Dinitrogen Complex with Siloxide Supporting Ligands
• Authors of publication: Mansell, Stephen M.; Farnaby, Joy H.; Germeroth, Anne I.; Arnold, Polly L.
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 15
• Pages of publication: 4214
• a: 16.1405 ± 0.0004 Å
• b: 17.105 ± 0.0004 Å
• c: 25.3526 ± 0.0006 Å
• α: 98.417 ± 0.002°
• β: 95.6393 ± 0.0019°
• γ: 117.137 ± 0.002°
• Cell volume: 6052.6 ± 0.3 ų
• Cell temperature: 170 ± 2 K
• Ambient diffraction temperature: 170 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0699
• Residual factor for significantly intense reflections: 0.0478
• Weighted residual factors for significantly intense reflections: 0.1044
• Weighted residual factors for all reflections included in the refinement: 0.1141
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No