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Information card for entry 4081159
Preview
Coordinates | 4081159.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C51 H34 Cl8 N3 O4 P Rh2 S2 |
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Calculated formula | C51 H34 Cl8 N3 O4 P Rh2 S2 |
Title of publication | Cyclometalation of Anthyridine-Based Ligands with Dirhodium Acetates: Structure and Catalytic Activity |
Authors of publication | Huang, Da-wei; Lo, Ying-Hao; Liu, Yi-Hung; Peng, Shie-Ming; Liu, Shiuh-Tzung |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 14 |
Pages of publication | 4009 |
a | 11.8618 ± 0.0004 Å |
b | 13.4211 ± 0.0004 Å |
c | 18.8676 ± 0.0006 Å |
α | 104.485 ± 0.003° |
β | 92.647 ± 0.002° |
γ | 111.303 ± 0.003° |
Cell volume | 2678.05 ± 0.17 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0687 |
Residual factor for significantly intense reflections | 0.0514 |
Weighted residual factors for significantly intense reflections | 0.1309 |
Weighted residual factors for all reflections included in the refinement | 0.1485 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.026 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4081159.html
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Users of the data should acknowledge the original authors of the
structural data.