Information card for entry 4081216

Structure parameters

• Formula: C37 H44 Ge N2 O2 W
• Calculated formula: C39.5 H42.5 Ge N2 O2 W
• Title of publication: Synthesis, Structure, and Reactivity of Tungsten Acetylide‒Germylene Complexes
• Authors of publication: Sakaba, Hiroyuki; Arai, Yasuhiro; Suganuma, Kensei; Kwon, Eunsang
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 18
• Pages of publication: 5038
• a: 33.805 ± 0.003 Å
• b: 14.2517 ± 0.001 Å
• c: 18.5822 ± 0.0013 Å
• α: 90°
• β: 104.291 ± 0.007°
• γ: 90°
• Cell volume: 8675.5 ± 1.2 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0597
• Weighted residual factors for all reflections included in the refinement: 0.1637
• Goodness-of-fit parameter for all reflections included in the refinement: 1.056
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No