Information card for entry 4081220

Structure parameters

• Formula: C64.5 H96 N2 O0.25 P2 Ru2 S2 Si6
• Calculated formula: C64.5 H96 N2 O0.25 P2 Ru2 S2 Si6
• Title of publication: Synthesis, Structure, and Reactivity of Trigonal Bipyramidal Ruthenium(IV) Trialkyl Complexes
• Authors of publication: Kwan Huang, Enrique; Cheung, Wai-Man; Chan, Sharon Lai-Fung; Sung, Herman H. Y.; Williams, Ian D.; Leung, Wa-Hung
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 16
• Pages of publication: 4483
• a: 20.1717 ± 0.0008 Å
• b: 19.8722 ± 0.0007 Å
• c: 20.4513 ± 0.0007 Å
• α: 90°
• β: 96.252 ± 0.004°
• γ: 90°
• Cell volume: 8149.3 ± 0.5 ų
• Cell temperature: 173 ± 0.14 K
• Ambient diffraction temperature: 173 ± 0.14 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0917
• Residual factor for significantly intense reflections: 0.0607
• Weighted residual factors for significantly intense reflections: 0.1409
• Weighted residual factors for all reflections included in the refinement: 0.1583
• Goodness-of-fit parameter for all reflections included in the refinement: 1.008
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No