Information card for entry 4081263

Structure parameters

• Formula: C43 H54 Ge N5 P
• Calculated formula: C43 H54 Ge N5 P
• Title of publication: Synthesis and Characterization of a 2,6-Diiminophenylgermanium(II) Hydroxide, Azide, and Triazaphospole
• Authors of publication: Chia, Siew-Peng; Li, Yongxin; So, Cheuk-Wai
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 18
• Pages of publication: 5231
• a: 12.8309 ± 0.0005 Å
• b: 20.87 ± 0.0009 Å
• c: 14.7922 ± 0.0006 Å
• α: 90°
• β: 98.06 ± 0.002°
• γ: 90°
• Cell volume: 3921.9 ± 0.3 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0843
• Residual factor for significantly intense reflections: 0.0626
• Weighted residual factors for significantly intense reflections: 0.1671
• Weighted residual factors for all reflections included in the refinement: 0.1789
• Goodness-of-fit parameter for all reflections included in the refinement: 1.093
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No