Information card for entry 4081312

Structure parameters

• Formula: C28 H35 Cl4 N3 O Pd
• Calculated formula: C28 H35 Cl4 N3 O Pd
• Title of publication: Reactivity Study of Imino-N-Heterocyclic Carbene Palladium(II) Methyl Complexes
• Authors of publication: Badaj, Anna C.; Lavoie, Gino G.
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 16
• Pages of publication: 4577
• a: 9.3459 ± 0.0012 Å
• b: 26.128 ± 0.004 Å
• c: 13.0359 ± 0.0017 Å
• α: 90°
• β: 95.764 ± 0.002°
• γ: 90°
• Cell volume: 3167.1 ± 0.8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0672
• Residual factor for significantly intense reflections: 0.0572
• Weighted residual factors for significantly intense reflections: 0.1128
• Weighted residual factors for all reflections included in the refinement: 0.1156
• Goodness-of-fit parameter for all reflections included in the refinement: 1.366
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No