Information card for entry 4081330

Structure parameters

• Formula: C56 H47 B Cl2 F24 N Os P
• Calculated formula: C56 H47 B Cl2 F23.997 N Os P
• Title of publication: Osmium Models of Intermediates Involved in Catalytic Reactions of Alkylidenecyclopropanes
• Authors of publication: Esteruelas, Miguel A.; López, Ana M.; López, Fernando; Mascareñas, José L.; Mozo, Silvia; Oñate, Enrique; Saya, Luc\?ía
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 17
• Pages of publication: 4851
• a: 19.056 ± 0.002 Å
• b: 17.482 ± 0.002 Å
• c: 34.82 ± 0.005 Å
• α: 90°
• β: 91.2683 ± 0.0019°
• γ: 90°
• Cell volume: 11597 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0936
• Residual factor for significantly intense reflections: 0.0837
• Weighted residual factors for significantly intense reflections: 0.1778
• Weighted residual factors for all reflections included in the refinement: 0.1819
• Goodness-of-fit parameter for all reflections included in the refinement: 1.098
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No